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Bio-inert Quaternary Pump User Manual 61
Optimizing Performance
5
Optimize the Compressibility Compensation Setting
Tab le 5 Solvent Compressibility
Solvent (pure) Compressibility (10-6/bar)
Acetone 126
Acetonitrile 115
Benzene 95
Carbon tetrachloride 110
Chloroform 100
Cyclohexane 118
Ethanol 114
Ethyl acetate 104
Heptane 120
Hexane 150
Isobutanol 100
Isopropanol 100
Methanol 120
1-Propanol 100
To l u e n e 8 7
Water 46
- Agilent 1260 Infinity 1
- Bio-inert Quaternary Pump 1
- In This Guide 3
- Contents 5
- Introduction 9
- Introduction to the Pump 10
- Hydraulic Path 12
- How Does the Pump Work? 13
- 1 Introduction 14
- Bio-inert Materials 17
- Early Maintenance Feedback 19
- Instrument Layout 20
- Agilent Technologies 21
- Site Requirements 22
- Power Cords 23
- Bench Space 24
- Condensation 24
- Physical Specifications 25
- Performance Specifications 26
- Installing the Pump 27
- Unpacking the Pump 28
- Accessory Kit 29
- One Stack Configuration 30
- 3 Installing the Pump 32
- EdlZghl^iX] 34
- CVbZeaViZ 34
- HiVijhaVbe 34
- HZg^VacjbWZg 34
- Connecting Modules 36
- Flow Connections of the Pump 38
- Priming the System 41
- Regular Priming 43
- Changing Solvents 44
- Using the Pump 47
- 4 Using the Pump 48
- Algae Growth in HPLC Systems 50
- Solvent Information 51
- Titanium 52
- Fused silica 52
- Optimizing Performance 55
- When to Use a Degasser 56
- 5 Optimizing Performance 58
- Choosing the Right Pump Seals 59
- Status Indicators 64
- Error Messages 64
- Test Functions 64
- System Pressure Test 65
- Module Status Indicator 67
- User Interfaces 68
- Agilent Lab Advisor Software 69
- Error Information 71
- 7 Error Information 72
- What Are Error Messages 73
- General Error Messages 74
- Remote Timeout 75
- Synchronization Lost 76
- Leak Sensor Open 77
- Leak Sensor Short 77
- Compensation Sensor Open 78
- Compensation Sensor Short 78
- Fan Failed 79
- Open Cover 79
- Module Error Messages 80
- Pressure Above Upper Limit 81
- Pressure Below Lower Limit 82
- Pressure Signal Missing 82
- Missing Pressure Reading 83
- Pump Configuration 83
- Valve Fuse 84
- Inlet-Valve Fuse 84
- Valve Failed (MCGV/SSV) 85
- Motor-Drive Power 86
- Encoder Missing 87
- Inlet-Valve Missing 87
- Temperature Out of Range 88
- Temperature Limit Exceeded 88
- Servo Restart Failed 89
- Pump Head Missing 89
- Index Limit 90
- Index Adjustment 90
- Index Missing 91
- Stroke Length 91
- Initialization Failed 92
- Wait Timeout 93
- Degasser: cannot read signal 94
- Degasser: limit not reached 94
- System Pressure Test failed 101
- Leak Rate Test 102
- Running the Test 104
- Evaluating the Results 104
- Maintenance 107
- Introduction to Maintenance 108
- Warnings and Cautions 109
- 9 Maintenance 110
- Overview of Maintenance 111
- Cleaning the Module 112
- Damage of the module 113
- Always filter solvents 113
- Exchanging the Outlet Valve 117
- KVakZXVe^aaVgn 118
- DjiaZikVakZ 118
- DjiaZiXVe^aaVgn 121
- Ejg\ZkVakZ 121
- LVhiZijWZ 121
- Ejbe]ZVYhXgZlh 124
- Seal Wear-in Procedure 125
- Maintenance of the Pump Head 126
- AdX`hXgZl 128
- EjbeYg^kZ 129
- Ejbe]ZVY 129
- W^d"^cZgi^YZci^[^Zg/ 129
- Zc\gVk^c\ 129
- 789^ciZg[VXZWdVgY 135
- Parts for Maintenance 137
- 10 Parts for Maintenance 138
- Outlet Valve 140
- Purge Valve Assembly 141
- Active Inlet Valve 142
- Figure 14 Active inlet valve 143
- Starter-Kit Bio-inert 145
- Solvent Cabinet 146
- Bottle Head Assembly 148
- System Tool Kit 151
- Preventive Maintenance Kit 152
- Identifying Cables 153
- Cable Overview 154
- Analog Cables 156
- Remote Cables 158
- 11 Identifying Cables 160
- BCD Cables 161
- CAN/LAN Cables 163
- External Contact Cable 164
- Agilent Module to PC 165
- Hardware Information 167
- Electrical Connections 168
- Rear View of the Module 169
- Interfaces 170
- Overview Interfaces 172
- >chigjbZci 174
- BVaZ ;ZbVaZ ;ZbVaZ BVaZ 174
- Special Interfaces 175
- 12 Hardware Information 176
- Special Settings 179
- Appendix 181
- General Safety Information 182
- Safety Symbols 184
- Abstract 185
- Batteries Information 186
- Radio Interference 187
- Sound Emission 188
- *G5611-90000* 194
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